Studies on the Spectral Interference of Gadolinium on Different Analytes by Inductively Coupled Plasma Atomic Emission Spectrometry

Influence of hydrogen gas over the interference of acids in inductively coupled plasma atomic emission spectrometry.

The effect of hydrogen gas on the plasma and its influence on acid interferences in plasma atomic emission spectrometry was studied. The study was performed with HCl and HNO(3) in the concentration range of 0-2 mol l(-1). Vanadium and magnesium were used as test elements, the study was extended to other several elements. The effects of hydrogen gas on the plasma were studied by measuring excita...

Inductively Coupled Plasma - Optical Emission Spectrometry

ACKNOWLEDGEMENTS INTRODUCTION CONTENTS 1.1 Forensic Science Investigations 1.2 Forensic Science Analysis 2 1.3 Inductively Coupled Plasma-Optical Emission Spectrometry 7 1.4 The Aims of This Investigation 8 2 INDUCTIVELY COUPLED PLASMA-OPTICAL EMISSION SPECTROMETRY 10 2 .l Introduction 2.2 The Inductively Coupled Plasma 2.3 Instrumentation Used in This Study 2.3.1 Radio Frequency Generator 2.3....

Inductively Coupled Plasma/Optical Emission Spectrometry

Selective Separation and Preconcentration of trace Amounts of Gallium in Water and Rice Samples using Cloud Point Extraction and Determination by Inductively Coupled Plasma-Atomic Emission Spectrometry

In the present study a cloud-point extraction process using non-ionic surfactant Triton X-114 for selective extraction of gallium from aqueous solutions was developed. The method is based on the complex formation of Ga (III) with N, N′ -bis (salycilidene)-1, 2-phenylenediamine (salophen) as a chelating agent in buffer media of pH 5. After phase separation and dilution of the surfactant-rich pha...

Determination of titanium and vanadium in Ziegler-Natta catalysts by inductively coupled plasma atomic emission spectrometry.

A method for the determination of Ti and V using inductively coupled plasma atomic emission spectrometry (ICP OES) in Ziegler-Natta polymerization catalysts is proposed. The concentrations of both Ti and V are efficiently determined after catalyst acid digestion with a mixture of HNO3 + HCl + HF and heating (160 degrees C for 6 h) or with 10% (v/v) H2SO4 and heating (160 degrees C for 6 h) or w...